The efficient synthesis of 3-R-6-thio-6,7-dihydro-2H-[1?2?4]triazino[2,3-c]-quinazoline-2-ones and their derivatives, antimicrobial and antifungal activity
The formation of the potassium salt of 3-substituted 6-thio-6,7-dihydro-2H-[1,2,4]triazino[2,3-C]quinazoline-2-ones in the presence of potassium hydroxide in alcohols via reaction of 6-R-3-(2-aminophenyl)-1,2,4-triazin-5-ones (2) with carbon disulfide.
Подобные документы
The novel approach to chemical design of carbon-coated Al2O3 nanoparticles with an average particle size of 8-10 nm was developed. Carbon coating was synthesised by modification of fumed alumina support with 4,4-methylenebis and its subsequent pyrolysis.
автореферат, добавлен 02.04.2014New facile method for the controllable synthesis of high quality single-phase nanowires with from nanowires templates. Detailed characterization of the superconducting and transport properties of nanowires. Synthesis of porous nanowires and nanotubes.
статья, добавлен 30.07.2016Investigations of nanoporous carbon materials from organic raw materials of vegetable nature appropriate to be used as an electrode component in supercapacitors with an aqueous electrolyte. Familiarization with voltammograms of experimental samples.
статья, добавлен 30.07.2016Features of the laboratory experiment with exposure to cadmium salt solution and growth processes peroxidise activity in seedlings Pinus Sylvestris. Features of influence of cadmium ions on peroxidise activity and accumulation of 15-day-old cultures.
статья, добавлен 27.10.2016The technology of obtaining and comparative tests of the medical enterosorbents, activated coal and lignin enterosorbents. High activity lignin enterosorbents at the treatment of lacto-dependent diarrhoea. Physical-chemical features of enterosorbents.
статья, добавлен 02.04.2014Microporous structure of outgoing and thermally modified plant-extracted carbon material. Porous system characteristics by different methods on low temperature adsorption-desorption. Сharacteristic of most effective thermal modifications form nanopores.
статья, добавлен 24.02.2016Reactions of Thiocyanate and Isothiocyanate Derivatives of Fluoroolefins with N-Nucleophilic Reagents. The Influence of the N-Nucleophile on the Construction of Six-Membered Heterocycles. The Use of Fluoroolefins with a Carbonyl-Containing Substitutent.
статья, добавлен 05.03.2013Benzisothiazolium Salts. Heterocyclic Annulated Isothiazolium Salts. Structure. X-ray Diffraction. Molecular Spectra. Analytical methods. Reactivity, general survey. Oxidation to Sultims and Sultams. Ring Transformation in Other Heterocyclic Compounds.
статья, добавлен 05.03.2013- 59. Algorithm of optimal solution search for the control with model system of methanol synthesis column
The mechanism of development and implementation of the optimal synthesis search algorithm and analysis of gas costs. Features of control using the maintenance schedule. Technological process of methanol synthesis under conditions close to optimal.
статья, добавлен 14.01.2017 Using of solid carbon in industrial branches. Analyzes of the unity of composition, molecular and supermolecular structure of shungite concentrate and silicon-carbon from rice hulls which provides their effective practical use in the same engineering.
статья, добавлен 02.04.2014Study of adsorption of cadmium (II) cations on the surface of macroporous amorphous silica with chemically modified b-cyclodextrin, its functional derivatives. The analysis of kinetic curves of sorption within the Lagergren model reaction pseudo order.
статья, добавлен 02.04.2014- 62. Preparation and properties of hybrid poly(3,4-ethylenedioxythiophene)–carbon nanotubes composites
It was investigated the infrared spectra of the hybrid composites poly. The current-voltage characteristics of the obtained materials. It is shown that increasing the content of carbon nanotubes leads to decrease of the resistance of hybrid films.
статья, добавлен 30.07.2016 Thiophene ring closure in pyridine derivatives. Syntheses of tri- and polycyclic systems based on thienopyridines. Pyridine ring closure in thiophene derivatives. Methods for the preparation of thieno[3,2-b]pyridine derivatives and their properties.
статья, добавлен 05.03.2013Study of influence of amino acids on the hydroxyapatite formation. Study of mineral obtained by transmission electron microscopy and powder X-ray diffraction. Analysis of the phase composition, crystal size and lattice microstrains of calcium phosphate.
статья, добавлен 23.12.2016- 65. Ti-Al alloy
A new process for developing titanium aluminides using chemical vapor synthesis was investigated in a laboratory experiment. Aluminum subchloride was used as the reducing agent in the reaction with TiCl4 and the source of aluminum for Ti-Al alloy.
лабораторная работа, добавлен 01.11.2019 Synthesis methods development of ionic liquids based on quaternary ammonium salts, their application as components of the polymeric electrolytes for electrochemical devices. Рroperties of liquids depending on the structure of cationic and anionic parts.
статья, добавлен 20.03.2014Obtaining JBW zeolite from hydrogels under hydrothermal conditions by alkaline reaction using NaOH as an activating agent. Orthorhombic space group Pmc21 with unit cell parameters, X-ray powder diffraction. Comprehensive study of the synthetic zeotype.
статья, добавлен 18.01.2021Two possible approaches to the phenothiazine ring that, to the authors’ knowledge, have not been explored yet. The attack of a nitrene onto a diary sulde, the "nitrogen equivalent" of the thionation reaction. The diene character of ve-membered rings.
научная работа, добавлен 05.03.2013Oxidized with solution of hydrogen peroxide multiwalled carbon nanotubes (MWCNTs) were modified with 2-hydroxyethylmethacrylate (HEMA) or chitosan (CTS). Morphology and surface properties of the pristine and modified MWCNTs have been investigated.
статья, добавлен 03.04.2014A three compounds, p-aminobenzylden-a-naftylamine and its metal complexes have been prepared. Studies have shown that the investigated metal complexes are effective inhibitors of the oxidation of complex action. Antioxidant effect of synthesized metal.
статья, добавлен 23.02.2021The technology for the synthesis of two coumarin-chalcone hybrids by means of Kleisen-Schmidt condensation between 3-acetylcoumarin with benzaldehyde and 4-chlorobenzaldehyde, respectively. Method of identification and control of a chemical process.
статья, добавлен 15.01.2021Critical reviews on "Heterocyclic Compounds" within topic-related volumes dealing with all aspects such as synthesis, reaction mechanisms, structure complexity, reactivity, stability, biology, pharmacological aspects, applications in material sciences.
учебное пособие, добавлен 05.03.2013The preparation methods, and main characteristics of known catalysts for carbon monoxide oxidation have been examined. A short review in a tabular form which facilitates a quick view on catalysts for CO oxidation (mainly cobalt ones) is represented.
статья, добавлен 30.08.2016A controlling the morphology of zinc hydroxide and zinc oxide at room temperature without using any template or surface ligand. Identify the precipitated materials. Dependence of ZnO morphology on Zn2+ concentration. Scanning electron microscopy of zinc.
статья, добавлен 30.07.2016Isomeric aminobenzoic acid – an important chemical product of organic synthesis used in the production of synthetic dyes, medicinal and aromatic substances, wines, pesticides. Investigation the reaction of the oxidization of 2- and 3-aminotoluenes.
статья, добавлен 22.03.2016